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Beilstein J. Org. Chem. 2016, 12, 1598–1607, doi:10.3762/bjoc.12.156
Graphical Abstract
Scheme 1: Comparison of early C–N and C–O coupling reactions.
Figure 1: General flow scheme for catalytic Chan–Lam reaction.
Figure 2: Observed trend for the effect of changing oxygen pressure on the NMR yield of 19.
Figure 3: Comparison of 1H NMR spectra of non-purified (top) and QP-DMA purified (bottom) continuous flow syn...
Scheme 2: Scope of the catalytic Chan–Lam reaction in continuous flow.
Scheme 3: Syntheses of substrate 39.
Figure 4: NOESY NMR spectrum for 30 with the characteristic NOESY signal encircled.
Figure 5: NOESY NMR spectrum for 33 with the characteristic NOESY signal encircled.
Figure 6: NOESY NMR spectrum for 35 with the characteristic NOESY signal encircled.
Figure 7: Substrates that gave no products in flow.
Scheme 4: Scale-up procedure for 19.